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The works of the highly experienced and famous chymist, John Rudolph Glauber

THE FIRST CENTURY: OR GLAUBER’S Wealthy Store-House of Treasures. (continued 2)

Christopher Packe translation

After that all the humidity is come forth, take the gourd (being cold) out of the sand, and pour some water on the matter that it may become soft, and that a Salt may be extracted from it, wherein the Gold lurketh, which was contained in the mine; coagulate the Lixivium being full of Gold, into a Red-Salt, the which by adding Litharge, is to be melted in such Crucibles which are not broken.

The Litharge draws the Gold unto it out of the Salt, which is to be separated from the Lead, after that manner which shall be shewn in the following Chapters or Treatises.

XLII. The preparation of a Water necessary for the extracting of Gold.

Take of this water of small charges, which thou shalt prepare plentifully without trouble, pour upon mines, and again separate it by distillation, to be again used in new labours, that there may be no need to prepare it again anew, because this doth not onely alwaies remain effectual, but also is increased in every operation: So that thou mayest be able to extract mines and minerals ad infinitum, if so be thou shalt prepare but one pound or pint at the first.

N. B. By this means all Gold how little soever it be, is plentifully extracted out of flints, sand, and any other minerals, without any cost excepting fire.

XLIII. Another water for extracting silver.

Take this water extracteth silver out of the poor mines of silver, sand, and stones; the operation of the same, is like the former one, and its increase is like the increase of the former water, so that after this manner silver may be plentifully extracted out of poor minerals, and no other cost is required besides fire.

N. B. Instead of may be taken since it performs the same thing in extracting, which the other performeth.

XLIV. Another easie manner of plentifully extracting gold, and silver out of poor minerals, it being of little or no cost.

Mix thou the mine or minerals with the requisite waters, fill with the same of good earth, set them near each other in a great put it in and distill the spirits, which pay all the charges, and which supply gold and silver without any costs, the which is to be received by lead.

XLV. Another more easie manner of extracting gold and silver out of minerals.

Mix the mine or mineral with the requisite waters, and moisten it by degrees, cast the whole into the spirits depart into a receiving vessel, and in the time of distillation, the gold and silver are dissolved by that dissolvant, the which being extracted, remain with or among and are rinced by water out of the mineral, so that they are attained without costs, and the spirits being collected in the receiving vessel, do recompence all charges.

XLVI. An easie operation of plentifull extracting gold and silver out of fat white Clay or Potters-earth.

Although gold and silver be extracted out of minerals by moist waters, by a troublesome operation as we have taught in the beginning, yet such an extraction brings no small profit, because they may be freed from those waters by precipitation; and those very waters do readily serve for the making or preparing of Salt Peter. With a fat Argilla or white Clay, the matter goes otherwise, because the spirit hath crept into the fat earth, and scarce a half part is received, unless the earth be first deprived of its fatness by making burning bright, it being that which doth also require its own peculiar labour.

Seeing that therefore in all places of the world, wheresoever earth is found, such fat white Clays containing gold and silver do plentifully offer themselves, and none hath been hitherto found, who hath indeavoured to extract and bring them to use, especially whenas they contain but little of gold or silver, not able to defray the charges of the lead bestowed.

I could not but open a very easie way of performing that thing with no small profit, the which is perfected by the following labour.

Mix such an earth containing gold or silver, with or of that greater one, and cast it by degrees into my first or second Distillatory Furnaces, and draw forth the spirits by distilling, that the solved gold or silver may remain in From that which is broken by a Mill or grinding is washed off with hot water, and is reduced by lead as is shewed before.

XLVII. After what manner by the help of art, gold may be easily and plenteously extracted from the sand of Granates, Agaths, Saphyrs, and Rubies, and other stoney Mineral earths, which do neither admit of fusion, nor Lead, nor sharp Waters.

It is certain that all Granates or Marbles, the red, black, ash-coloured, duskish, also of whatsoever colour they are, or wheresoever they are found, whether in Brooks or Rivers, or in Sand, or fat Earth, or in high Rocks, do always contain much of Gold, but that by reason of their glassy nature, they cannot be tamed by Aq. fortis’s, and by reason of their most difficult fusion cannot be wrought by Saturn or Lead; for that cause they have made none partaker of their gold, and they have been neglected as unprofitable earths, whenas notwithstanding they being handled by little labour, they are able to afford much gold.

Some one therefore may ask, because they cannot be subdued either by lead or Aquæ fortis’s, what course must be taken, that gold may be extracted out of their bowels? I answer. and also by a Fusible they may be so overcome, that the gold which they have may be withdrawn from them with profit, for because they can bear the fire, they are and perform by a double labour, one through their sharpness, and another by reason of a strong fire, so that nothing is safe from so great forces, but all things are constrained to yield unto so great violence. Hence they do willingly afterwards enter the Salt of Lead, and in time of melting do readily draw out their gold.

XLVIII. A most firm demonstration, that sharp Waters and Salts after the manner of the ways hitherto described, do draw forth more Gold and Silver as it were without cost, out of Mines or Minerals containing Gold and Silver, than sumptuous or costly melting Fires.

It is not unknown to every one that is seasoned but even with a mean knowledge of gold bearing Mines, that without the addition of Lead or other flowable things, Gold can in no wise be melted out of them, whenas therefore there is little Gold in those, and nevertheless much of Lead or other matters is required to be added for an easie fusion or melting sake, who shall be fit for the undergoing of so great costs? Hence it hath come to pass that such poor minerals could bring nothing of profit in common.

It being also granted, that there is so much of Gold and Silver in Minerals, that they will defray the charges of fire and fusion, and afford Gold and Silver with profit, yet such operations are not comparable to my inventions using Waters and Salts, no more than as Water to Wine, or Night to Day.

For first, fusion or melting far exceeds in its costs the extraction which is perfected by Salt and Waters. And then it can never be brought to pass that fusion should expell all the Gold and Silver out of Mines and Minerals, but leaves some thereof in the drosses, next also there is made a loss of all the volatile Gold and Silver, which are cast forth by a most strong fire, and driven away into the air; on the contrary, of the more ample and wealthy profits, which the extraction of Gold and Silver out of Minerals bringeth, this is not the least, that not onely all the Gold and Silver which is fixed, is drawn out without any detriment or loss, but also those two metals being as yet volatile are extracted at once and made fixt and constant in the fire, whenas notwithstanding by the vehemence of a melting fire, they are wholly dispersed and reduced into nothing. For the Waters of Salts do fix the volatile fugative spirits of Gold and Silver, the which by the vehement blasts of Bellows, are rendred as yet far more volatile, so that by the help of fusion scarce half the Gold is gotten which the extraction by the Waters of Salt affordeth.

Add to this, that not onely all the Silver and Gold, as well the volatile as the fixt is gotten together without any loss, but also the charges of Coals are far less, and one operatour may perform as much of this extraction of Gold and Silver, as three in the labour of fusion or melting.

From hence it is easily to be seen, how much profit and fruit may be gained by this my most excellent invention in all places of Germany. For this extraction is not onely for extracting Gold and Silver as well out of rich as poor Mines, but also snatcheth out all the Gold and Silver, in Flints tinged with any colour, wherewith all Brooks, Rivers, and Fields are filled.

Now follow some particular transmutations of the imperfect Metals into more perfect ones, by common fire, and Crude Salt, and by the not common con-centred moist fire of Salt.

XLIX. A fundamental and evident demonstration, that a true transmutation, or trans-changing of Metals may be exercised in all places of the earth, wheresoever Men may dwell, yea in the least Cottages of Countrey folks, and indeed by the same matters and vessels which are found in them.

It is well known, that even the poorest and vilest or meanest Countrey can want neither fire, nor salt, nor earthen vessels, necessary for the boyling of Meats. Therefore being furnished with Salt, a piece of Copper of some old Kettle shall easily supply him, the which it shall be free for him, by fire and salt to trans-change into a better and more noble body, but because Man hath a far better and commodious Salt for the transmutation of Metals in his possession, which excells common Salt in its goodness, he may of right and worthily make use of his own proper Salt before a strange and foreign one, and that after this manner.

Boil thy own, or the Urine of another man, to the consistancy of Honey, in which decoction, all the unprofitable moisture of the Urine departs by exhalation, and the Salt thereof remains in the Kettle or earthen Pot; admix thou with this condensed Urine, so much of Calx-vive, or the ashes of burnt Woods, that it may come into a thick or gross lump. But thin plates of Copper cut in pieces, and purged by making them bright burning hot ought to be in readiness, and also an earthen Pot having its Cover, wherein let that mass of Urine, and Calx-vive, together with the thin plates of Copper be put; when thou hast all these things in a readiness, mix the Urine as abovesaid with the Calx or slack-lime or ashes, and fill thy Pot to the height of three or four fingers, upon which put some of the plates of Copper, and so stratum super-stratum till the Pot is full, then cover it with its Cover, which thou shalt well fence with Lute made of Meal, Water, and Paper, that not any vapour at all may come forth. For assoon as the Calx-vive is mixed with the condensed or co-thickned Urine, the Spirit of Urine begins to operate by its own proper efficacy, and therefore it is necessary that the Cover be straightway laid on the Pot, and be fenced with a due Lute or Clay; the Pot being thus filled and cover’d, set it aside in some certain place for the space of half a year, in which time the spirit of Urine being stirred up by the Calx-vive, displays its virtues on the Copper, and exalts it into a higher degree, as that it is tinged of a skie and green colour mixed, and is rendred fit for the Painters Art; one pound whereof is more worth than two or three pounds of Copper, one pound whereof doth for the most part render one pound with four or five ounces of this colour, and so it affords a profitable transmutation of Copper.

L. After what manner, out of this partly Green, partly Skie-colour of Copper, Gold and Silver is to be separated.

He that desires to separate Gold and Silver out of this colour, whereof no great masses are attained, but onely and alone whereby it is demonstrated that the thing may be done, he must use the following operation.

First, he must take good heed in taking the colour out of the earthen Pot, lest any thing of the mass of the Urine, and Calx be mixed with the beautifull colour, and render it impure.

The thin plates being taken out, they are to be often crookedly bowed, and moved upwards and downwards, that the colour may fall off from the plates like scales. The remaining Copper which is not yet turned into colour, is reserved for a new labour; to be repeated after the same manner. Wine-vinegar is poured on the colour, or the sharp water of Tartar extracted after the Distillation of adust Wine from its Lees, with water by decoction, and it is to be so long boiled in a Copper Kettle, or an earthen Pot glazed, till all the colour shall be solved; the Solution being cast into a Filtre, the Vinegar or Water of Tartar onely passeth through, and a reddish powder is left in the Filtre, the which being melted with Lead in a Cupel, after the exhalation of the Lead, it leaves a grain of Gold. For the spirit of Urine hath ripened somewhat of the Copper into Gold, which the Vinegar or Water of Tartar did not dissolve but left, attracting onely the Copper by solution. And because somewhat of Silver is ripened in the Copper through this same operation, and is dissolved with the Copper, by the Vinegar or Water of Tartar, something of common Salt is to be added to the Water of Tartar or Vinegar, that the Silver may not be solved by the same, but may remain with the Calx of Gold, and may be retained with the same.

N. B. Pure and clear Vinegar ought to be taken for this labour, if you would preserve the colour unhurt, for after some part of the Vinegar is evaporated away, the green colour of the Copper grows together into fair green small stones, one pound whereof is more to be esteemed than five or six pounds of Verdi grease, which is sold in the Shops.

This artificial operation therefore affords a beautifull and christalline vitriol of Venus, and some small quantity of Gold and Silver; whereof although there be not so great plenty that it may bring profit, yet it shews the possibility of the thing, and teacheth that a transmutation of Metals, may be exercised in any small Cottage by any Countrey Man.

But if any one shall collect Urine, and extract from thence the volatile spirit of its Salt by Distillation, he shall far more deeply pierce the heart of the Copper, and shall obtain more of Gold and Silver than he can get by the but now mentioned rustical labour, of which matter more things are found in other places of my Writings.

LI. After what sort pure Gold may be extracted out of any Copper.

In all Copper a spiritual occult Gold lies hid, the which in the labour of separation by Lead in a Cupel or Test, is not taken notice of, or considered. But this very Gold is nothing else but the colour of Copper, so firmly adhering unto its body, that it remaineth very difficult to be separated from thence, but the operation being rightly instituted, although it be not gainfull, yet it demonstrates a possibility of the thing, for the sake of experiencing whereof, to wit, whether there be Gold in all Copper, thou must labour after the following manner.

Dissolve Copper in Aq. Regis, and pour much water on the solution, that by this water the dissolved Copper may be largely diffused. Into this solution diffused by the water, pour Lead that is dissolved in Aq. Fortis, so that one or two half ounces of Lead may answer to one pound of Copper. But as often as the Lead shall settle to the bottom, thou shalt shake or stir it, that the solution may be well mixed, and that the Lead may attract something of Gold; and may precipitate it with it self to the bottom, the which being dried and separated in a Cupel, will leave a small quantity of Gold, not for an argument of profit, but a token of a possibility, which testifies that there is Gold in all Copper. But if any thing of profit were to be received, such Copper was to be taken which was already changed into vitriol. But among vitriols the Hungarian, Cyprian, Indian, Japanick, and other the like do excell, which do offer themselves in the Mines of Gold-bearing Copper, and are handled after the following manner.

LII. The manner of extracting Gold out of natural vitriol.

Dissolve thou vitriol in common water, and pour on the vitriol dissolved, a littled of dissolved Lead, and stir both solutions by frequent motions, that the Lead may attract the Gold out of the vitriol, to be dried and separated by a Cupel, which will remain like a grain of greater or lesser quantity, as the vitriol shall contain more or less of the same.

Of the vitriolated water out of which the Gold was extracted, thou shalt again make vitriol by so long boiling, and evaporating till a thin skin appear, which being then exposed to the cold will shoot into Crystals. But this operation brings with it more profit, if it be not now boiled up into Crystals, but that vitriol onely be taken which is drawn out of its Mineral into Water, and after the extraction of the Gold, is at length boiled up into vitriol.

But least this fishing of Gold out of vitriol should seem wonderfull unto any, we will shew a way, whereby Gold may be extracted out of Sea Water, or Sea Salt, the solution of Lead assisting: The manner is as followeth.

LIII. After what manner Gold is to be extracted out of Sea Salt, or Sea Water, not indeed with profit, but onely that it may be demonstrated, that Gold is hidden even in Sea Water or Sea Salt.

Fill a great Copper Kettle with Sea Water, and pour thereon a little dissolved Lead; the which goes to the bottom because it cannot indure Salt, and is straightway precipitated into a white powder, move and stir the water in the Kettle often, that the solution of Lead may every where touch the Sea-Salt-Water.

Through this action, a spiritual Gold adheres to the leaden powder, and sinks to the bottom together with it, which powder being freed from its Salt by common Water, and dried, and melted in a Cupel, leaves a small grain of Gold, as a remainder.

N. B. For this fishing Silver is more fit than Lead.

LIV. How, out of poor Mines of Copper, from which no profit can be perceived, Copper, as also Gold it self if it be present, is to be easily and without costs, extracted and separated.

The sandy or sulphurous Mine or Mineral of Copper is to be roasted or calcined, by burning even to the consuming of the Sulphur, because sharp waters do not assault sulphureous matters, the Mineral being calcined and beaten into a powder, fill a gourd, and pour our solving secret on the same, the which I have taught above at the extracting of Minerals.

The whole dissolvent in abstracting or distilling is recovered, and that indeed not without increase. But the Copper and Silver do stick fast in the dissolved Salt, which remained in the Mineral after the abstraction, and the which is to be washed out with water, out of which water, which drew out that Salt, the Gold contained therein, may by the solution of Lead or Silver, be drawn forth.

But if the same water be boiled untill a thin skin appear at the top, and exposed to the cold, it will shoot into a green vitriol, but for the extracting the Copper out of the Salt-Water, Rods of Iron are to be put therein, which do attract the Copper, the which being withdrawn and washed clean, and melted into Copper by fusion, is administred for other uses: For because it is like to a tender and filed powder, it is changed by an easie business into Verdi-grease, after the manner which shall by and by be taught.

LV. After what manner Gold may by an easie business by Fire and Salt, be separated out of Copper.

If Gold shall be mixed with a mass or lump of Copper, all the Copper is to be reduced in a bright burning Fire into Ashes: and the Ashes are to be infused in our secret Aceum or Vinegar, the which dissolveth the Copper onely by decoction, and leaveth the Gold undissolved, like a shining powder, to be dried and melted with Borace, out of which Gold of twenty three Caracts proceedeth.

That Vinegar, our secret Aceum, draws all the Copper from the golden Calx. The Copper is separated from the Vinegar by Rods of Iron, being laid therein as we have taught in the foregoing manner.

LVI. How Copper being extracted out of vitriolated Water, and adhering to Rods of Iron, is to be changed into Verdi-grease.

This pure Copper may be moistened with the strongest Vinegar, and put into earthen Pots, the which being covered with its Cover well fenced with Clay, are to be placed in Horse dung, and to be left therein for a time, yet so as that the heap of Dung be sometimes renewed. All the Copper is in a short time changed into Verdi-grease, and indeed far more pure than that which is set forth to Sale in the Shops, and which is made in Spain, by the husks or pressed out of clusters of Grapes.

N. B. In extracting Copper out of Mines, regard is to be had unto this thing, to wit, that with poor and wild or course veins of Copper, Lapis Calaminaris, or Zink is sometimes found to be admixed; which is no ways perceived to be in them. But if those Minerals are extracted with Aq. Regis, and this be to be taken away by Distillation, none of the Aq. Regis goes forth, but onely a flegm without savour, because the Lapis Calaminaris or Zink doth retain all the Acrimony with it, just as if those two Minerals should say to the Aq. Regis, we do not as yet let thee go, because as yet, we have need of thy indeavour for our amendment, &c.

But it is certain that whatsoever Minerals and Metals do retain with them sharp spirits, are as yet immature, and may be ripened by those spirits, that they may bestow Gold and Silver, as hath been already said, and shall as yet more largely be spoken to.

LVII. Out of wild or course Minerals, or veins of Lead, admitting of no melting, out of which no good Lead, much less Gold or Silver, can be drawn, how to extract not onely Lead, but also Gold and Silver with profit.

As we have said above, that some Minerals or Veins of Copper do appear in Mines, the which by reason of Lapis Calaminaris or Zink do refuse all melting, and can be by no fire reduced: So also we here admonish, that Minerals of Lead are found, the which do indeed contain much Lead, but by reason of the Lapis Calaminaris, Zink, and a sulphureous Sand being admixed with them, they cannot be overcome by any melting, for these matters do take away a ready flowing from the Lead, and do cause that such Minerals, which for the most part together with Lead, do also hide not a little of Gold and Silver, are cast away as altogether unfit, and unprofitable, whenas notwithstanding very much profit might be received from them after this manner.

Let the Mineral by pounding be broken in small pieces, and in my little secret Furnace which I have fitted for the calcining of Minerals, let it be roasted with bright burning Coals, that the gross Sulphur may conceive a flame, and burn. If in time of operation the matter should gather it self into heaps or knobs, and in co-heaping should make round Pellets, it being taken out of the Furnace, let it again be beaten, be set upon live Coals and roasted, and these labours be so often repeated, untill all the Sulphur shall be consumed, and the Mineral doth no longer co-heap it self into knobs, but being made bright burning hot like dead ashes; it no longer sends forth a sulphureous stink. At length out of these ashes being well washed, a dead and unprofitable matter separates its self from the good and metallick earth, the which being melted by it self in a Furnace called by the Germans Stichofen, becomes a flowable Lead which containeth Gold and Silver.

But if the Mineral be so stubborn that it altogether refusing all melting, could not by it self be reduced, and nevertheless contain Gold and Silver, something of Litharge is to be added to that metallick earth, which procures a flux unto it, and yields that Gold and Silver bearing Lead, which by the common operation wholly refuseth to offer it self.

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