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A text-book of assaying

Note 106 — Chapter XVII

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It is difficult to get ferric chloride free from arsenic; but the following treatment will remove 80 or 90 per cent. of the arsenic contained in the commercial material:—Dissolve 2 or 3 lbs. of ferric chloride with the smallest amount of water that will effect solution with the addition of 100 c.c. of hydrochloric acid; add a solution of sulphurous acid in quantity sufficient to reduce 2 or 3 per cent. of the iron to the ferrous state; allow to stand a week; and then boil, to remove the hydrochloric acid added. Nitric acid, which is prejudicial, is also removed by this treatment.

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